2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

Base Information

Chemical Name:2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid
CAS No.:1300720-73-3
Molecular Formula:C₃₁H₃₄F₃N₅O₈
Molecular Weight:661.635
Hs Code.:

2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

Synonyms:2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

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Chemical Property of 2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

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Technology Process of 2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

There total 3 articles about 2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 652967-34-5
C₂₀H₂₁NO

: 174091-56-6
5-trifluoroacetamido-2,6-anhydro-9-azido-3,5,9-trideoxy-D-glycero-D-galactonon-2-enoic acid

: 1300720-73-3
2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; dimethyl sulfoxide; tert-butyl alcohol; at 20 ℃; for 24h;
DOI:10.1002/asia.201000594

Reference yield:

: 1300720-55-1
methyl 2,6-anhydro-3,5-dideoxy-9-O-(p-tosyl)-5-trifluoroacetamido-D-glycero-D-galactonon-2-enonate

: 1300720-73-3
2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 6 h / 70 °C

2: sodium hydroxide / water / 0.33 h / 20 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide; tert-butyl alcohol / 24 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/asia.201000594

Reference yield:

: 41976-65-2
methyl 2,6-anhydro-3,5-dideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enonate

: 1300720-73-3
2,6-anhydro-9-{4-[2((4'-ethylbiphen-4-yl)carboxamido)prop-2-yl]-1H-1,2,3-triazol-1-yl}-3,5,9-trideoxy-5-trifluoroacetamido-D-glycero-D-galactonon-2-enoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 24 h / 0 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 6 h / 70 °C

3: sodium hydroxide / water / 0.33 h / 20 °C

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide; tert-butyl alcohol / 24 h / 20 °C

With pyridine; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/asia.201000594