2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid

Base Information

• Chemical Name: 2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid
• CAS No.: 16933-69-0
• Molecular Formula: C₉H₁₃NO
• Molecular Weight: 151.208
• Mol file: 16933-69-0.mol

Synonyms:2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid

Chemical Property of 2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid

There total 3 articles about 2-(Cyclohexen-⁽¹⁾-yl)-propen-⁽²⁾-saeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-ethynyl-1-chlorocyclohexane (6209-75-2) → 2-(Cyclohexen-(1)-yl)-propen-(2)-saeureamid (16933-69-0)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

2: diethyl ether

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;

DOI:10.1021/jo01272a005

Reference yield:

isocyanate de chlorosulfonyle (1189-71-5) + vinylidenecyclohexane (5664-20-0) → 2-(Cyclohexen-(1)-yl)-propen-(2)-saeureamid (16933-69-0)

Guidance literature:

In diethyl ether;

DOI:10.1021/jo01272a005

Reference yield:

→ 2-(Cyclohexen-(1)-yl)-propen-(2)-saeureamid (16933-69-0)

Guidance literature:

C6H11=C=CH2, Chlorsulfonylisocyanat (Tab.I), neben 2-Azetidinon;

DOI:10.1021/ja00967a041

upstream raw materials:

isocyanate de chlorosulfonyle

vinylidenecyclohexane

1-ethynyl-1-chlorocyclohexane

Downstream raw materials:

2-cyclohexylpropanamide