4-bromo-N-(diphenylethenylidene)aniline

Base Information

Chemical Name:4-bromo-N-(diphenylethenylidene)aniline
CAS No.:29376-76-9
Molecular Formula:C20H14 Br N
Molecular Weight:348.242
Hs Code.:
Mol file:29376-76-9.mol

Synonyms:Aniline,p-bromo-N-(diphenylvinylidene)- (7CI,8CI); Benzenamine,4-bromo-N-(diphenylethenylidene)- (9CI); N-p-Bromophenyl-2,2-diphenylvinylideneamine;NSC 409239

Suppliers and Price of 4-bromo-N-(diphenylethenylidene)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-bromo-N-(diphenylethenylidene)aniline

Chemical Property:

Vapor Pressure:6.03E-09mmHg at 25°C
Boiling Point:481°C at 760 mmHg
Flash Point:244.7°C
Density:1.21g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-bromo-N-(diphenylethenylidene)aniline

There total 2 articles about 4-bromo-N-(diphenylethenylidene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1871-76-7
diphenylacetic acid chloride

: 14987-96-3
N-(4-bromophenyl)triphenyliminophosphorane

: 29376-76-9
4-bromo-N-(2,2-diphenylvinylidene)aniline

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 0.25h;
DOI:10.1002/ejoc.201500704

Reference yield:

: 117-34-0
2,2-diphenylacetic acid

: 29376-76-9
4-bromo-N-(2,2-diphenylvinylidene)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Reflux

2: triethylamine / 1,2-dichloro-ethane / 0.25 h / 20 °C

With thionyl chloride; triethylamine; In 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201500704

Reference yield: 95.0%

: 29376-76-9
4-bromo-N-(2,2-diphenylvinylidene)aniline

: 221044-05-9
N-(2-pyrimidyl)indole

: N-(1-(1H-indol-2-yl)-2,2-diphenylvinyl)-N-(pyrimidin-2-yl)-4-bromoaniline

Guidance literature:: With dimanganese decacarbonyl; In toluene; at 130 ℃; for 10h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.8b00204