benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

Base Information

Chemical Name:benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate
CAS No.:1052240-89-7
Molecular Formula:C₂₉H₃₀N₂O₂S
Molecular Weight:470.635
Hs Code.:

Synonyms:benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

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Chemical Property of benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

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Technology Process of benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

There total 1 articles about benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1052240-88-6
benzyl 2-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-2-thioxoethylcarbamate

: 106-95-6
allyl bromide

: 1052240-89-7
benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

Guidance literature:: benzyl 2-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-2-thioxoethylcarbamate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

allyl bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol801657q

Reference yield:

: 1052240-89-7
benzyl (R)-1-((2R,5R)-2,5-diphenylpyrrolidin-1-yl)-1-thioxopent-4-en-2-ylcarbamate

: C₂₉H₃₀N₂O₃

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 1h; optical yield given as %de;
DOI:10.1021/ol801657q