threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester

Base Information Edit

Chemical Name:threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester
CAS No.:88854-18-6
Molecular Formula:C₁₅H₁₉NO₅
Molecular Weight:293.32
Hs Code.:
Mol file:88854-18-6.mol

Synonyms:threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester Edit

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Technology Process of threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester

There total 12 articles about threo-O-Acetyl-N-acetyl-β-phenylserine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (E)-ethyl 2-acetamido-3-acetoxy-3-phenylacrylate

: 88854-18-6,101310-94-5
(2S,3R)-ethyl 2-acetamido-3-acetoxy-3-phenylpropanoate

Guidance literature:: With (1R,1’R,2S,2’S)-2,2’-di-tert-butyl-2,3,2’,3’-tetrahydro-1H,1‘H-(1,1‘)biisophosphindolyl; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; In dichloromethane; at 20 ℃; for 24h; under 22801.5 Torr; Reagent/catalyst; Solvent; Pressure; enantioselective reaction; Catalytic behavior; Autoclave;
DOI:10.1039/c7cc03902f

Reference yield: 97.0%

: -ethyl-2-acetamido-3-acetoxy-3-phenyl acrylate

: 88854-18-6,101310-94-5
(2S,3R)-ethyl 2-acetamido-3-acetoxy-3-phenylpropanoate

Guidance literature:: With (S)-di-1-adamantylphosphino(tert-butylmethylphosphino)methane(1,5-cyclooctadiene)rhodium(I) hexafluoroantimonate; hydrogen; In methanol; for 1h; under 2280.15 Torr; enantioselective reaction; Catalytic behavior;
DOI:10.1021/acs.orglett.9b02702