methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

Base Information

Chemical Name:methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate
CAS No.:949167-01-5
Molecular Formula:C₁₇H₂₅FN₂O₄
Molecular Weight:340.395
Hs Code.:

Synonyms:methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

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Chemical Property of methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

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Technology Process of methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

There total 1 articles about methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 149437-67-2
5-(4-fluorophenyl)-5-oxopentanoic acid methyl ester

: 949167-01-5
methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

Guidance literature:: t-butoxycarbonylhydrazine; 5-(4-fluorophenyl)-5-oxopentanoic acid methyl ester; In isopropyl alcohol; for 6h; Heating / reflux;

With hydrogen; platinum(IV) oxide; In isopropyl alcohol; at 20 ℃; for 8h; under 2660.18 Torr;

Reference yield:

: 949167-01-5
methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate

: 949167-02-6
tert-butyl [2-(4-fluorophenyl)-6-oxopiperidin-1-yl]carbamate

Guidance literature:: methyl 5-(N'-tert-butoxycarbonylhydrazino)-5-(4-fluorophenyl)pentanoate; With hydrogenchloride; sodium hydroxide; In methanol; at 20 ℃; for 2h;

With hydrogenchloride; water; In methanol;

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;