1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

Base Information

Chemical Name:1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene
CAS No.:87405-96-7
Molecular Formula:C₁₂H₁₁Cl₂F₅
Molecular Weight:321.117
Hs Code.:

Synonyms:1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

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Chemical Property of 1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

Chemical Property:

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Technology Process of 1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

There total 1 articles about 1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-82-8
Isopropylbenzene

: 87405-96-7
1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / aluminium chloride / 8 h / 120 °C

2: 60 percent / thionyl chloride / pyridine / 24 h / Heating

With aluminium trichloride; thionyl chloride; pyridine;
DOI:10.1016/S0022-1139(00)81231-2

Reference yield: 69.0%

: 87405-96-7
1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

: 87406-02-8
1,1,3,3,3-pentafluoro-2-<4-(1-methylethyl)phenyl>propene

Guidance literature:: With zinc(II) chloride; zinc; In methanol; at 35 - 40 ℃; for 44h;
DOI:10.1016/S0022-1139(00)81231-2

Reference yield:

: 87405-96-7
1-(1,2-Dichloro-2,2-difluoro-1-trifluoromethyl-ethyl)-4-isopropyl-benzene

: 4-(1-methylethyl)-α-(trifluoromethyl)benzeneacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / Zn, ZnCl₂ / methanol / 44 h / 35 - 40 °C

2: 1.) NaOC₂H₅; 2.) 58 percent HI, acetic acid / 1.) 25 deg C, 1 h; 2.) 18 h, reflux

With hydrogen iodide; sodium ethanolate; acetic acid; zinc(II) chloride; zinc; In methanol;
DOI:10.1016/S0022-1139(00)81231-2