(1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime

Base Information

• Chemical Name: (1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime
• CAS No.: 1227781-75-0
• Molecular Formula: C₁₉H₁₇NO₂
• Molecular Weight: 291.349
• Mol file: 1227781-75-0.mol

Synonyms:(1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime

Chemical Property of (1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime

There total 1 articles about (1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

O-allylhydroxylamine hydrochloride (38945-21-0) + 1-(4-methoxy-phenyl)-3-phenyl-propynone (16616-43-6) → (1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime (1227781-75-0)

Guidance literature:

With pyridine; sodium sulfate; In methanol; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ol100803e

Reference yield: 88.0%

(1Z)-1-(4-methoxyphenyl)-3-phenyl-2-propyn-1-one O-(2-propenyl)oxime (1227781-75-0) → 5-(4-methoxyphenyl)-3-phenyl-4-(2-propen-1-yl)isoxazole (1227781-93-2)

Guidance literature:

With gold(III) chloride; In trans-1,2-dichloroethylene; at 20 ℃; regioselective reaction; Inert atmosphere; Reflux;

DOI:10.1021/ol100803e

upstream raw materials:

O-allylhydroxylamine hydrochloride

1-(4-methoxy-phenyl)-3-phenyl-propynone

Downstream raw materials:

5-(4-methoxyphenyl)-3-phenyl-4-(2-propen-1-yl)isoxazole