S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

Base Information

Chemical Name:S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate
CAS No.:1392881-20-7
Molecular Formula:C₁₃H₁₀BrF₅O₂S
Molecular Weight:405.183
Hs Code.:

Synonyms:S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

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Chemical Property of S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

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Technology Process of S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

There total 4 articles about S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1416359-96-0
C₁₆H₈Br₂F₆S₂

: 67-64-1
acetone

: 1392881-20-7
S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

Guidance literature:: C₁₆H₈Br₂F₆S₂; acetone; With potassium hydride; In tetrahydrofuran; at 0 ℃;

With trifluoroacetic acid; In water; Reflux;
DOI:10.1016/j.bmcl.2013.08.108

Reference yield:

: C₁₆H₉Br₂F₇S₂

: 1392881-20-7
S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; tetrabutylammomium bromide / dichloromethane; water

2: potassium hydride / tetrahydrofuran / 0 °C

3: water; trifluoroacetic acid / Reflux

With tetrabutylammomium bromide; water; potassium hydride; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm301076q

Reference yield:

: 1416359-96-0
C₁₆H₈Br₂F₆S₂

: 1392881-20-7
S-(4’-bromophenyl)-4-oxo-2-(pentafluoroethyl)pentanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydride / tetrahydrofuran / 0 °C

2: water; trifluoroacetic acid / Reflux

With water; potassium hydride; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm301076q