tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

Base Information

Chemical Name:tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate
CAS No.:1420764-46-0
Molecular Formula:C₂₁H₃₀O₇S
Molecular Weight:426.531
Hs Code.:

Synonyms:tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

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Chemical Property of tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

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Technology Process of tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

There total 4 articles about tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1420764-40-4
1-bromomentyl-2,6-bis(tert-butoxycarbonylmethoxy)benzene

: 10387-40-3
potassium thioacetate

: 1420764-46-0
tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

Guidance literature:: In acetone; at 20 ℃; Inert atmosphere;
DOI:10.1002/cssc.201200572

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 1420764-46-0
tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 2 h / 60 °C / Inert atmosphere

1.2: 48 h / Reflux; Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: acetone / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In tetrachloromethane; acetone;
DOI:10.1002/cssc.201200572

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1420764-46-0
tert-butyl 2-{2-[(acetylsulfanyl)methyl]-3-[2-(tert-butoxy)-2-oxoethoxy]phenoxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 2 h / 60 °C / Inert atmosphere

1.2: 48 h / Reflux; Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: acetone / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In tetrachloromethane; acetone;
DOI:10.1002/cssc.201200572