benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

Base Information

Chemical Name:benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate
CAS No.:196794-47-5
Molecular Formula:C₃₂H₄₃ClN₂O₈
Molecular Weight:619.155
Hs Code.:

Synonyms:benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

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Technology Process of benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

There total 10 articles about benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 37755-48-9,40298-04-2
benzyl (2S)-2-hydroxy-4-methylpentanoate

: 196794-35-1
(R)-3-[(R)-2-tert-Butoxycarbonylamino-3-(3-chloro-4-methoxy-phenyl)-propionylamino]-2-methyl-propionic acid

: 196794-47-5
benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

Guidance literature:: With dicyclohexyl-carbodiimide;
DOI:10.1021/jo971645t

Reference yield:

: (S)-2-((R)-3-Amino-2-methyl-propionyloxy)-4-methyl-pentanoic acid benzyl ester; compound with trifluoro-acetic acid

: 162465-45-4
(R)-2-((tet-butoxycarbonyl)amino)-3-(3-chloro-4-methoxyphenyl)propanoic acid

: 196794-47-5
benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; at 0 - 20 ℃; for 21h;
DOI:10.1002/chem.200500282

Reference yield:

: 162465-45-4
(R)-2-((tet-butoxycarbonyl)amino)-3-(3-chloro-4-methoxyphenyl)propanoic acid

: 245125-89-7
(S)-2-((R)-3-Amino-2-methyl-propionyloxy)-4-methyl-pentanoic acid benzyl ester

: 196794-47-5
benzyl (2S)-2-[(2R)-3-[(2R)-2-tert-butoxycarbonylamino-3-(3-chloro-4-methoxyphenyl) propionylamino]-2-methylpropionyloxy]-4-methylpentanoate

Guidance literature:: With N-[3-(diethylamino)propyl]-N'-ethylcarbodiimide hydrochloride; benzotriazol-1-ol; triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo9907585