(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

Base Information

Chemical Name:(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene
CAS No.:229027-14-9
Molecular Formula:C₃₉H₆₂O₃Si
Molecular Weight:607.005
Hs Code.:

Synonyms:(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

Chemical Property:

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Technology Process of (2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

There total 3 articles about (2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 77-76-9
2,2-dimethoxy-propane

: 229027-13-8
(E)-(2R,3S)-1-(tert-Butyl-diphenyl-silanyloxy)-icos-4-ene-2,3-diol

: 229027-14-9
(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1016/S0040-4020(99)00163-5

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 229027-14-9
(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 10 h

2: 82 percent / camphorsulfonic acid / CH₂Cl₂ / 10 h / Ambient temperature

With 1H-imidazole; camphor-10-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00163-5

Reference yield:

: 229027-12-7
(E)-(2R,3S)-Icos-4-ene-1,2,3-triol

: 229027-14-9
(2R,3S)-1-tert-butyldiphenylsilyloxy-2,3-isopropylidenedioxyeicos-4(E)-ene

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 10 h

2: 82 percent / camphorsulfonic acid / CH₂Cl₂ / 10 h / Ambient temperature

With 1H-imidazole; camphor-10-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00163-5