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Technology Process of 2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

Base Information
  • Chemical Name:2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine
  • CAS No.:1071519-86-2
  • Molecular Formula:C28H42Br2N2O8
  • Molecular Weight:694.458
  • Hs Code.:
2,3-bis(bromomethyl)-N<sub>1</sub>,N<sub>1</sub>,N<sub>4</sub>,N<sub>4</sub>-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

Synonyms:2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

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Chemical Property of 2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine
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Technology Process of 2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

There total 1 articles about 2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N<sub>1</sub>,N<sub>1</sub>,N<sub>4</sub>,N<sub>4</sub>-tetrakis(tert-butoxycarbonyl)-2,3-dimethylbenzene-1,4-diamine
1071519-82-8

N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)-2,3-dimethylbenzene-1,4-diamine

2,3-bis(bromomethyl)-N<sub>1</sub>,N<sub>1</sub>,N<sub>4</sub>,N<sub>4</sub>-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine
1071519-86-2

2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

Guidance literature:
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 2h; Irradiation;
DOI:10.1021/ol8018067

Reference yield:

2,3-bis(bromomethyl)-N<sub>1</sub>,N<sub>1</sub>,N<sub>4</sub>,N<sub>4</sub>-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine
1071519-86-2

2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine

4-methoxy-aniline
104-94-9

4-methoxy-aniline

C<sub>42</sub>H<sub>58</sub>N<sub>4</sub>O<sub>10</sub>

C42H58N4O10

Guidance literature:
4-methoxy-aniline; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h;
2,3-bis(bromomethyl)-N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)benzene-1,4-diamine; In N,N-dimethyl-formamide; mineral oil; at 70 ℃; for 3h;
DOI:10.1021/ol8018067
upstream raw materials:

N1,N1,N4,N4-tetrakis(tert-butoxycarbonyl)-2,3-dimethylbenzene-1,4-diamine

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