4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile

Base Information

• Chemical Name: 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile
• CAS No.: 1571757-24-8
• Molecular Formula: C₃₀H₃₃ClN₂O₃
• Molecular Weight: 505.057
• Mol file: 1571757-24-8.mol

Synonyms:4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile

Chemical Property of 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile

There total 2 articles about 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4,5-dichloro-3,6-bis(hexyloxy)phthalonitrile + β-naphthol (135-19-3) → 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile (1571757-24-8) + 3,6-bis-(hexyloxy)-4,5-bis(naphthalen-2-yloxy)phthalonitrile

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 8h; Inert atmosphere; Heating;

DOI:10.1016/j.dyepig.2016.10.014

Reference yield: 42.0%

4,5-dichloro-3,6-bis(hexyloxy)phthalonitrile + β-naphthol (135-19-3) → 4-chloro-5-bis(2-naphthoxy)-3,6-bis-(hexyloxy)phthalonitrile (1571757-24-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 45 ℃; for 50h;

DOI:10.1016/j.jorganchem.2013.12.044

upstream raw materials:

β-naphthol