1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

Base Information

Chemical Name:1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene
CAS No.:1453905-02-6
Molecular Formula:C₁₇H₁₈INO₅
Molecular Weight:443.238
Hs Code.:

Synonyms:1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

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Chemical Property of 1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

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Technology Process of 1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

There total 4 articles about 1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1453905-05-9
2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-methylphenylmethanol

: 1453905-02-6
1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/chem.201301298

Reference yield:

: 53413-67-5
6-nitroveratrylbromide

: 1453905-02-6
1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / 20 °C

3: triphenylphosphine; 1H-imidazole; iodine / dichloromethane / 4 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; iodine; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201301298

Reference yield:

: 613-84-3
2-hydroxy-5-methylbenzaldehyde

: 1453905-02-6
1-((2-(iodomethyl)-4-methylphenoxy)methyl)-4,5-dimethoxy-2-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / 20 °C

3: triphenylphosphine; 1H-imidazole; iodine / dichloromethane / 4 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; iodine; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201301298