N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine

Base Information

• Chemical Name: N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine
• CAS No.: 1426958-17-9
• Molecular Formula: C₂₀H₂₆BNO₂
• Molecular Weight: 323.243
• Mol file: 1426958-17-9.mol

Synonyms:N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine

Chemical Property of N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine

There total 13 articles about N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-benzylidene benzylamine (780-25-6) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine (1426958-17-9)

Guidance literature:

With rare-earth metal amido complexe-[(κ²-N,O-κ¹-(1-(C₆H₅CON=CH₂CH₂)-3-(CH₃)3C₆H₂(N(CH)₂NC)))₂REN(SiMe₃)₂]; In toluene; at 110 ℃; for 6h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/acs.inorgchem.8b02067

Reference yield: 32.0%

N-benzylbenzamide (1485-70-7) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine (1426958-17-9) + N-benzylidene benzylamine (780-25-6)

Guidance literature:

With bis(trimethylsilyl)amide yttrium(III); In toluene; at 100 ℃; for 24h; Temperature; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/acs.orglett.9b04606

Reference yield:

N,N-dibenzyl-4-cyanophenylamide (1372314-22-1) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → N,N-dibenzyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-amine (1426958-17-9) + 4-(((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)oxy)methyl)benzonitrile + N,N-dibenzylamine hydrochloride (20455-68-9)

Guidance literature:

With tris((4,4-dimethyl-2-oxazolinyl)phenylborate) MgMe; In benzene-d6; at 20 ℃; for 15h;

DOI:10.1021/acscatal.5b01038

upstream raw materials:

N-benzylidene benzylamine

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

benzaldehyde

benzylamine

Downstream raw materials:

dibenzylamine

tribenzylamine

N,N-dibenzyl-1-(4-(trifluoromethyl)phenyl)methanamine

N,N-dibenzyl-1-(thiophen-2-yl)methanamine