Technology Process of C42H50F2O4
There total 6 articles about C42H50F2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
at 80 ℃;
for 3.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide / tetrakis(triphenylphosphine) palladium(0) / toluene; diisopropylamine / 7 h / 40 °C
2.1: hydrogen / 5%-palladium/activated carbon / toluene / 24 h / 100 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -70 °C
3.2: 4 h / 20 °C
4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3.5 h / 80 °C
With
copper(l) iodide; hydrogen; sodium carbonate; lithium diisopropyl amide;
tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; diisopropylamine; toluene;
4.1: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / 5%-palladium/activated carbon / toluene / 24 h / 100 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -70 °C
2.2: 4 h / 20 °C
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 3.5 h / 80 °C
With
hydrogen; sodium carbonate; lithium diisopropyl amide;
tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; toluene;
3.1: Suzuki Coupling;