C₁₅H₂₂Cl₂O₂Si

Base Information

Chemical Name:C₁₅H₂₂Cl₂O₂Si
CAS No.:1520156-96-0
Molecular Formula:C₁₅H₂₂Cl₂O₂Si
Molecular Weight:333.33
Hs Code.:

C<sub>15</sub>H<sub>22</sub>Cl<sub>2</sub>O<sub>2</sub>Si

Synonyms:C₁₅H₂₂Cl₂O₂Si

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Chemical Property of C₁₅H₂₂Cl₂O₂Si

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Technology Process of C₁₅H₂₂Cl₂O₂Si

There total 3 articles about C₁₅H₂₂Cl₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1520156-93-7
C₁₅H₂₄Cl₂O₂Si

: 1520156-96-0
C₁₅H₂₂Cl₂O₂Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo402167q

Reference yield:

: 130217-38-8
2-(((tert-butyldimethylsilyl)oxy)methyl)-4,5-dichlorobenzaldehyde

: 1520156-96-0
C₁₅H₂₂Cl₂O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / 20 °C

2.1: borane-THF / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

2.2: 3 h / 0 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With borane-THF; potassium tert-butylate; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo402167q

Reference yield:

: 1520156-90-4
C₁₅H₂₂Cl₂OSi

: 1520156-96-0
C₁₅H₂₂Cl₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With borane-THF; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo402167q