10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Base Information

Chemical Name:10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine
CAS No.:107672-83-3
Molecular Formula:C₃₀H₂₇NO₆S
Molecular Weight:529.613
Hs Code.:

Synonyms:10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

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Chemical Property of 10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

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Technology Process of 10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

There total 4 articles about 10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 100-52-7
benzaldehyde

: 107672-79-7,155857-35-5
10-methoxy-6(4'-methoxy-benzo-2'-hydrothiophen-3'-on-S,S-dioxido)-5-methyl-3,4,6,7-tetrahydro-5H-furo(4.3.2-fg)-⁽³⁾-benzazacine

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: With ammonium chloride; acetic acid; for 8h; Heating;
DOI:10.1007/BF00780573

Reference yield:

: 107672-82-2
5-benzylidene-2-thiolen-4-one 1,1-dioxide

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / benzene / 3 h / Ambient temperature

2: 1) NaOMe; 2) NH₄Cl / aq. ethanol

With sodium methylate; ammonium chloride; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87458-5

Reference yield:

: 115-37-7
thebaine

: 107672-83-3,155857-36-6
10-methoxy-6-<7'-(4'-methoxy-2'-benzylidenebenzothiophen-3'-one-1',1'-dioxido)>-5-methyl-3,4,6,7-tetrahydro-5H-furo<4,3,2-f,g><3>benzazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / benzene / 3 h / Ambient temperature

2: 1) NaOMe; 2) NH₄Cl / aq. ethanol

With sodium methylate; ammonium chloride; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87458-5