phenyl acetate labelled at carbonyl group

Base Information

Chemical Name:phenyl acetate labelled at carbonyl group
CAS No.:92350-03-3
Molecular Formula:C₈H₈O₂
Molecular Weight:137.139
Hs Code.:

Synonyms:phenyl acetate labelled at carbonyl group

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Chemical Property of phenyl acetate labelled at carbonyl group

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Technology Process of phenyl acetate labelled at carbonyl group

There total 1 articles about phenyl acetate labelled at carbonyl group which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1520-57-6
[1-13C]acetyl chloride

: 108-95-2,27073-41-2
phenol

: 92350-03-3
phenyl acetate labelled at carbonyl group

Guidance literature:: With trifluorormethanesulfonic acid; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/acs.orglett.7b02052

Reference yield: 43.0%

: 92350-03-3
phenyl acetate labelled at carbonyl group

: 2-hydroxyacetophenone labelled at carbonyl

Guidance literature:: With aluminum (III) chloride; at 220 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.7b02052

Reference yield:

: 92350-03-3
phenyl acetate labelled at carbonyl group

: (E)-1-(2-hydroxyphenyl)-3-phenyl(1-13C)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / 12 h / 220 °C / Inert atmosphere; Sealed tube

2: sodium hydroxide / water; ethanol / 20 h / 20 °C

With aluminum (III) chloride; sodium hydroxide; In ethanol; water;
DOI:10.1021/acs.orglett.7b02052