2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone

Base Information

• Chemical Name: 2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone
• CAS No.: 83570-33-6
• Molecular Formula: C₂₂H₂₆O₅
• Molecular Weight: 370.445

Synonyms:2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone

Chemical Property of 2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone

Chemical Property:

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Technology Process of 2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone

There total 1 articles about 2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-chloro-3-cyclohexylnaphthalene-1,4-dione (83570-32-5) + (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol (100-79-8,36543-79-0) → 2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone (83570-33-6)

Guidance literature:

With sodium hydride; In paraffin; for 1.5h; Ambient temperature;

Reference yield: 62.0%

2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone (83570-33-6) → 5-cyclohexyl-10b,2-epoxymethano-2,3-dihydronaphtho<1,2-b>dioxin-6(10bH)-one (83570-35-8)

Guidance literature:

With hydrogenchloride; In methanol; at 0 ℃; for 1.5h;

Reference yield: 5.0%

2-cyclohexyl-3-(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,4-naphthoquinone (83570-33-6) → 5-cyclohexyl-10b,2-epoxymethano-2,3-dihydronaphtho<1,2-b>dioxin-6(10bH)-one (83570-35-8) + 5-cyclohexyl-10b,3-epoxymethano-2,3-dihydronaphtho<1,2-b>dioxin-6-(10bH)-one

Guidance literature:

With hydrogenchloride; In methanol; for 16h; Title compound not separated from byproducts; Heating;

upstream raw materials:

2-chloro-3-cyclohexylnaphthalene-1,4-dione

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

Downstream raw materials:

5-cyclohexyl-10b,2-epoxymethano-2,3-dihydronaphtho<1,2-b>dioxin-6(10bH)-one

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