3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Base Information

• Chemical Name: 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane
• CAS No.: 1369957-05-0
• Molecular Formula: C₂₀H₂₅N₅
• Molecular Weight: 335.452

Synonyms:3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Chemical Property of 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Chemical Property:

Purity/Quality:

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Technology Process of 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

There total 4 articles about 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-phenylmethyl-2-[(4-phenyl-1,2,3-triazol-1-yl)methyl]aziridine (1369956-93-3) + N,N-dimethylammonium chloride (506-59-2) → 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane (1369957-05-0)

Guidance literature:

With dimethyl amine; In acetonitrile; at 140 ℃; for 2h; regioselective reaction; Microwave irradiation;

DOI:10.3762/bjoc.7.205

Reference yield:

phenylacetylene (536-74-3) → 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane (1369957-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide / acetonitrile / 16 h / 20 °C / Reflux

2: dimethyl amine / acetonitrile / 2 h / 140 °C / Microwave irradiation

With copper(l) iodide; dimethyl amine; In acetonitrile;

DOI:10.3762/bjoc.7.205

Reference yield:

2-azidomethyl-1-(phenylmethyl)aziridine (1369956-88-6) → 3-dimethylamino-2-(phenylmethyl)amino-1-(4-phenyl-1,2,3-triazol-1-yl)propane (1369957-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide / acetonitrile / 16 h / 20 °C / Reflux

2: dimethyl amine / acetonitrile / 2 h / 140 °C / Microwave irradiation

With copper(l) iodide; dimethyl amine; In acetonitrile;

DOI:10.3762/bjoc.7.205

upstream raw materials:

2-azidomethyl-1-(phenylmethyl)aziridine

1-phenylmethyl-2-[(4-phenyl-1,2,3-triazol-1-yl)methyl]aziridine

N,N-dimethylammonium chloride

phenylacetylene

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