Technology Process of 5,6-bis[(5',5''-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]indane
There total 1 articles about 5,6-bis[(5',5''-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]indane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
Co2(CO)8;
In
1,4-dioxane; toluene;
under N2; Zn complex and Co2(CO)8 were dissolved in toluene/dioxane (5/1) and heated to 100°C, soln. of 1,6-heptadiyne and Co2(CO)8 in toluene was added dropwise (17 h); soln. was evapd. to dryness, residue was chromd. (silica gel, hexanes/THF (3/2));
DOI:10.1021/ja012489h