bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

Base Information

Chemical Name:bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne
CAS No.:402505-19-5
Molecular Formula:C₉₀H₈₆N₈O₈Zn₂
Molecular Weight:1538.5
Hs Code.:

Synonyms:bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

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Chemical Property of bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

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Technology Process of bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

There total 1 articles about bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 402505-25-3
(5-bromo-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)

: 402508-67-2
(5-ethynyl-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)

: 402505-19-5
bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

Guidance literature:: With As(C₆H₅)3; (C₂H₅)3N; Pd₂(C₆H₅CHCHCOCHCHC₆H₅)3; In tetrahydrofuran; triethylamine; under N2; Zn complexes, Pd complex and As(C6H5)3 were dissolved in 5:1 THF/triethylamine (5/1), the mixt. was stirred for 3 h at 40°C; solvent was evapd., residue was chromd. (silica gel, hexanes/THF (1/1)) followed by (SX-1 biobeads, THF);
DOI:10.1021/ja012489h

Reference yield: 94.0%

: 2396-63-6
hepta-1,6-diyne

: 402505-19-5
bis[(5,5'-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

: 402505-21-9
5,6-bis[(5',5''-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]indane

Guidance literature:: With Co₂(CO)8; In 1,4-dioxane; toluene; under N2; Zn complex and Co2(CO)8 were dissolved in toluene/dioxane (5/1) and heated to 100°C, soln. of 1,6-heptadiyne and Co2(CO)8 in toluene was added dropwise (17 h); soln. was evapd. to dryness, residue was chromd. (silica gel, hexanes/THF (3/2));
DOI:10.1021/ja012489h