3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Base Information

Chemical Name:3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene
CAS No.:1353897-40-1
Molecular Formula:C₄₂H₄₄N₆O₁₁
Molecular Weight:808.845
Hs Code.:

Synonyms:3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Suppliers and Price of 3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

There total 5 articles about 3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1353897-39-8
3,4-di-O-{1-[1(S)-methoxycarbonyl-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

: 1353897-40-1
3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Guidance literature:: With water; lithium hydroxide; In methanol; at 20 ℃; for 3h;
DOI:10.1039/c1ob06242e

Reference yield:

: C₃₀H₅₀O₇Si₂

: 1353897-40-1
3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 12 h / 20 °C

3: acetyl chloride / methanol / 12 h / 20 °C

4: water; lithium hydroxide / methanol / 3 h / 20 °C

With copper(ll) sulfate pentahydrate; water; sodium hydride; sodium L-ascorbate; acetyl chloride; lithium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06242e

Reference yield:

: 1353897-37-6
3,4-di-O-propynyl-2,6-O-TBDMS-C-glucosyl 1,4-dimethoxynaphthalene

: 1353897-40-1
3,4-di-O-{1-[1(S)-carboxy-2-phenylethyl]-4-methyl-1H-1,2,3-triazol-4-yl}-β-D-glucopyranosyl 1,4-dimethoxynaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 12 h / 20 °C

2: acetyl chloride / methanol / 12 h / 20 °C

3: water; lithium hydroxide / methanol / 3 h / 20 °C

With copper(ll) sulfate pentahydrate; water; sodium L-ascorbate; acetyl chloride; lithium hydroxide; In methanol; dichloromethane; water;
DOI:10.1039/c1ob06242e