2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

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Chemical Name:2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole
CAS No.:1443234-63-6
Molecular Formula:C₄₈H₄₈BrN₃O₂S₄
Molecular Weight:907.096
Hs Code.:

Synonyms:2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

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Chemical Property of 2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

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Technology Process of 2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

There total 5 articles about 2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 201802-29-1
N,N'-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

: 1443234-60-3
2,6-bis(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

: 1443234-63-6
2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In water; N,N-dimethyl-formamide; at 100 ℃; for 1h; Schlenk technique; Inert atmosphere; Microwave irradiation;
DOI:10.1002/ejoc.201201629

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1443234-63-6
2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; bis(pinacol)diborane / N,N-dimethyl-formamide / 80 °C / Schlenk technique; Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; N,N-dimethyl-formamide / 1 h / 100 °C / Schlenk technique; Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; caesium carbonate; bis(pinacol)diborane; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201629

Reference yield:

: 1010811-82-1
2,6-bis-(4-hexylthiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

: 1443234-63-6
2-(4-hexyl-5-(4-(bis(4-methoxyphenyl)amino)phen-1-yl)thiophen-2-yl)-6-(4-hexyl-5-bromothiophen-2-yl)benzo[1,2-d;4,5-d']bisthiazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / chloroform; acetic acid / 4 h / 20 °C / Schlenk technique; Inert atmosphere; Darkness

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; N,N-dimethyl-formamide / 1 h / 100 °C / Schlenk technique; Inert atmosphere; Microwave irradiation

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In chloroform; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201629