Technology Process of 3-benzyl-6-phenyl 1,2,3-oxathiazinane 2,2-dioxide
There total 6 articles about 3-benzyl-6-phenyl 1,2,3-oxathiazinane 2,2-dioxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-(Benzylamino)-1-phenyl-1-propanol;
With
1H-imidazole; thionyl chloride; triethylamine;
In
dichloromethane;
at 0 ℃;
With
sodium periodate; ruthenium(III) chloride trihydrate;
In
water; acetonitrile;
at 0 ℃;
for 2h;
DOI:10.1002/anie.200905329
- Guidance literature:
-
With
sodium periodate; ruthenium(III) trichloride hydrate;
In
water; acetonitrile;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/chem.201203825
- Guidance literature:
-
Multi-step reaction with 6 steps
1: n-butyllithium / tetrahydrofuran; hexane / 2.25 h / -78 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran; hexane / 2 h / 0 °C / Inert atmosphere
3: ethanol / 2 h / 25 °C / Inert atmosphere
4: sodium tetrahydroborate / ethanol / 4 h / 0 - 25 °C / Inert atmosphere
5: triethylamine; thionyl chloride; 1H-imidazole / dichloromethane / 2 h / 0 °C / Inert atmosphere
6: ruthenium(III) trichloride hydrate; sodium periodate / water; acetonitrile / 2 h / 0 °C / Inert atmosphere
With
1H-imidazole; sodium tetrahydroborate; sodium periodate; lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; ruthenium(III) trichloride hydrate; triethylamine;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201203825
