4-chlorocinnamyl isocyanate

Base Information

Chemical Name:4-chlorocinnamyl isocyanate
CAS No.:132606-72-5
Molecular Formula:C₉H₆ClNO
Molecular Weight:179.606
Hs Code.:

Synonyms:4-chlorocinnamyl isocyanate

Suppliers and Price of 4-chlorocinnamyl isocyanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorocinnamyl isocyanate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 4-chlorocinnamyl isocyanate

There total 4 articles about 4-chlorocinnamyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83421-78-7
(E)-3-(4-Chloro-phenyl)-acryloyl azide

: 132606-72-5
4-chlorocinnamyl isocyanate

Guidance literature:: In toluene; for 1h; Heating;
DOI:10.1021/jm00142a024

Reference yield:

: 35086-79-4,95602-71-4
cinnamoyl chloride

: 132606-72-5
4-chlorocinnamyl isocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / H₂O / 1 h / 0 °C

2: toluene / 1 h / Heating

With sodium azide; In water; toluene;
DOI:10.1021/jm00142a024

Reference yield:

: 1615-02-7,940-62-5
3-(4-chlorophenyl)prop-2-enoic acid

: 132606-72-5
4-chlorocinnamyl isocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; diphenyl phosphoryl azide / toluene / 3 h / 20 °C / Cooling with ice

2: benzine / Reflux

With diphenyl phosphoryl azide; triethylamine; In benzine; toluene; 2: |Curtius Rearrangement;
DOI:10.1080/00397911.2013.878360