3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

Base Information

Chemical Name:3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone
CAS No.:148680-83-5
Molecular Formula:C₂₈H₄₀O₄
Molecular Weight:440.623
Hs Code.:

Synonyms:3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

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Chemical Property of 3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

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Technology Process of 3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

There total 9 articles about 3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 100052-60-6
5,5-dimethyl-3-isopropoxy-2-cyclohexenone

: 148680-82-4
C₁₇H₂₃IO₂

: 148680-83-5
3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -78 deg C, 1 h; 2.) rt, 2 days;

Reference yield:

: 148680-79-9
C₁₅H₁₇BrO₂

: 148680-83-5
3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / n-butyl lithium / -78 °C

2: H₂ / Raney Ni

3: I₂, imidazole, Ph₃P

4: 42 percent / LDA / tetrahydrofuran / -78 °C

With 1H-imidazole; n-butyllithium; hydrogen; iodine; triphenylphosphine; lithium diisopropyl amide; nickel; In tetrahydrofuran;
DOI:10.1016/0040-4039(94)85070-4

Reference yield:

: 148680-75-5
C₁₃H₁₄O₄

: 148680-83-5
3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

Guidance literature:: Multi-step reaction with 8 steps

1: bromine, sodium acetate / acetic acid

2: K₂CO₃ / acetone

3: tetrahydrofuran

4: toluene sulfonic acid / benzene / Heating

5: 75 percent / n-butyl lithium / -78 °C

6: H₂ / Raney Ni

7: I₂, imidazole, Ph₃P

8: 42 percent / LDA / tetrahydrofuran / -78 °C

With 1H-imidazole; n-butyllithium; hydrogen; bromine; iodine; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; lithium diisopropyl amide; nickel; In tetrahydrofuran; acetic acid; acetone; benzene;
DOI:10.1016/0040-4039(94)85070-4