4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

Base Information

Chemical Name:4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol
CAS No.:161710-96-9
Molecular Formula:C₂₆H₃₈O₃
Molecular Weight:398.586
Hs Code.:

Synonyms:4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

There total 5 articles about 4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 187025-65-6
4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenone

: 161710-96-9
4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at 0 ℃; for 0.833333h;

Reference yield:

: 148680-83-5
3-isopropoxy-5,5-dimethyl-6-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-2-cyclohexenone

: 161710-96-9
4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / tetrahydrofuran; diethyl ether / 2.5 h / Ambient temperature

2: 80 percent / CeCl₃*7H₂O, NaBH₄ / methanol / 0.5 h / 0 °C

With sodium tetrahydroborate; cerium(III) chloride; In tetrahydrofuran; methanol; diethyl ether;

Reference yield:

: 100052-60-6
5,5-dimethyl-3-isopropoxy-2-cyclohexenone

: 161710-96-9
4-[2-(3,4-cyclohexylidenedioxy-5-isopropyl)phenyl]ethyl-3,5,5,trimethyl-2-cyclohexenol

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / 1.) LDA 1N / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) rt, 2 days

2: 99 percent / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature

3: 80 percent / CeCl₃*H₂O, NaBH₄ / methanol / 0.83 h / 0 °C

With sodium tetrahydroborate; cerium(III) chloride; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether;