(2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone

Base Information

• Chemical Name: (2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone
• CAS No.: 1258391-72-8
• Molecular Formula: C₂₆H₃₁BrCl₂O₈
• Molecular Weight: 622.337
• Mol file: 1258391-72-8.mol

Synonyms:(2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone

Chemical Property of (2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone

There total 1 articles about (2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(2,6-dibromo-3,5-bis(methoxymethoxy)phenyl)(3,5-dichloro-2-methoxy-6-(methoxy-methoxy)-4-methylphenyl)methanone (1258391-70-6) + prenyl bromide (870-63-3) → (2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone (1258391-72-8)

Guidance literature:

(2,6-dibromo-3,5-bis(methoxymethoxy)phenyl)(3,5-dichloro-2-methoxy-6-(methoxy-methoxy)-4-methylphenyl)methanone; With phenyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

prenyl bromide; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1002/anie.201003755

Reference yield: 56.0%

(2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone (1258391-72-8) + formic acid ethyl ester (109-94-4) → (2-formyl-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone (1258391-74-0)

Guidance literature:

(2-bromo-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone; With n-butyllithium; lithium chloride; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

formic acid ethyl ester; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1002/anie.201003755

upstream raw materials:

(2,6-dibromo-3,5-bis(methoxymethoxy)phenyl)(3,5-dichloro-2-methoxy-6-(methoxy-methoxy)-4-methylphenyl)methanone

prenyl bromide

Downstream raw materials:

(2-formyl-3,5-bis(methoxymethoxy)-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-methoxy-6-(methoxymethoxy)-4-methylphenyl)methanone