ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

Base Information

Chemical Name:ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate
CAS No.:1225032-67-6
Molecular Formula:C₂₅H₂₂Br₂ClNO₆
Molecular Weight:627.714
Hs Code.:

Synonyms:ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

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Chemical Property of ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

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Technology Process of ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

There total 6 articles about ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1225032-38-1
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

: 1225032-67-6
ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 - 10 ℃;

Reference yield:

: 1225032-65-4
3,5-dibromo-4-(4-methoxyphenoxy)benzaldehyde oxime

: 1225032-67-6
ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

2.1: Eaton′s Reagent / 16 h / 95 °C

3.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

3.2: 0.17 h / 20 - 25 °C

4.1: methanol / 2 h

With Eaton′s Reagent; boron tribromide; caesium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 855264-88-9
3,5-dibromo-4-(4-methoxy-phenoxy)-benzaldehyde

: 1225032-67-6
ethyl 2-(((3,5-dibromo-4-(3-((4-chlorophenyl)(hydroxy)methyl)-4-hydroxyphenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydroxylamine hydrochloride / ethanol; water / 2 h / 90 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

3.1: Eaton′s Reagent / 16 h / 95 °C

4.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

4.2: 0.17 h / 20 - 25 °C

5.1: methanol / 2 h

With Eaton′s Reagent; hydroxylamine hydrochloride; boron tribromide; caesium carbonate; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;