Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

Base Information

Chemical Name:Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate
CAS No.:1225032-38-1
Molecular Formula:C₂₅H₂₀Br₂ClNO₆
Molecular Weight:625.698
Hs Code.:

Synonyms:Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

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Chemical Property of Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

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Technology Process of Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

There total 6 articles about Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1225032-37-0
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

: 1225032-38-1
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-methoxy phenoxy)benzylidene)amino)oxy)propanoate; With boron tribromide; In dichloromethane; at -70 - -20 ℃; Inert atmosphere;

With water; In dichloromethane; at 20 - 25 ℃; for 0.166667h;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1225032-38-1
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 130 - 135 °C

2.1: hydroxylamine hydrochloride / ethanol; water / 2 h / 90 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

4.1: Eaton′s Reagent / 16 h / 95 °C

5.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

5.2: 0.17 h / 20 - 25 °C

With Eaton′s Reagent; hydroxylamine hydrochloride; boron tribromide; potassium carbonate; caesium carbonate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1225032-66-5
ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

: 1225032-38-1
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Eaton′s Reagent / 16 h / 95 °C

2.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

2.2: 0.17 h / 20 - 25 °C

With Eaton′s Reagent; boron tribromide; In dichloromethane;