2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

Base Information

Chemical Name:2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester
CAS No.:375394-32-4
Molecular Formula:C₁₉H₂₈N₂O₄Si
Molecular Weight:376.528
Hs Code.:

Synonyms:2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

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Chemical Property of 2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

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Technology Process of 2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

There total 2 articles about 2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 375394-11-9
2-(trimethylsilanylmethylamino)-pent-4-ene carboxylic acid methyl ester

: 375394-32-4
2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In acetonitrile; at 0 - 20 ℃;
DOI:10.1021/jo010144b

Reference yield:

: 50299-15-5,70837-19-3,81136-73-4,105929-46-2
allylglycine methyl ester

: 375394-32-4
2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃; KI / acetonitrile / 12 h / 83 °C

2: 45 percent / 1-hydroxy-7-azabenzotriazole; diisopropyl carbodiimide; diisopropylethylamine / acetonitrile / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; sodium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; diisopropyl-carbodiimide; In acetonitrile;
DOI:10.1021/jo010144b

Reference yield:

: 375394-32-4
2-[(2-Benzoylamino-acetyl)-trimethylsilanylmethyl-amino]-pent-4-enoic acid methyl ester

: (2R,4R)-1-(2-Benzoylamino-acetyl)-4-methyl-pyrrolidine-2-carboxylic acid methyl ester

: (2R,4S)-1-(2-Benzoylamino-acetyl)-4-methyl-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: With biphenyl; 9,10-Dicyanoanthracene; In methanol; acetonitrile; Title compound not separated from byproducts.; UV-irradiation;
DOI:10.1021/jo010144b