C₁₇H₁₅NO₃

Base Information

• Chemical Name: C₁₇H₁₅NO₃
• CAS No.: 1255087-75-2
• Molecular Formula: C₁₇H₁₅NO₃
• Molecular Weight: 281.311
• Mol file: 1255087-75-2.mol

Synonyms:C₁₇H₁₅NO₃

Chemical Property of C₁₇H₁₅NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₇H₁₅NO₃

There total 1 articles about C₁₇H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) → C17H15NO3 (1255087-75-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In water;

DOI:10.1039/C8CC08985J

Reference yield: 64.0%

C17H15NO3 (1255087-75-2) + 4-hydroxy-4-(trifluoromethyl)-2,5-cyclohexadien-1-one (113281-23-5) → N-[(3R,3aS,7aS)-3-(3-methoxybenzyl)-2,5-dioxo-7a-(trifluoromethyl)-2,3,3a,4,5,7a-hexahydrobenzofuran-3-yl]benzamide

Guidance literature:

4-hydroxy-4-(trifluoromethyl)-2,5-cyclohexadien-1-one; With C₂₄H₂₀B^(1-)*C₅₂H₇₈N₈O₂*H⁽¹⁺⁾; In dichloromethane; at 30 ℃; for 0.5h; Inert atmosphere;

C₁₇H₁₅NO₃; In dichloromethane; at -10 ℃; for 72h; enantioselective reaction; Inert atmosphere;

DOI:10.1039/C8CC08985J

Reference yield:

ethanol-d6 (1516-08-1) + C17H15NO3 (1255087-75-2) → C19H20(2)HNO4 (1255087-86-5) + C19H20(2)HNO4

Guidance literature:

With Bis-HQN-SQA; In dichloromethane; at 20 ℃; for 15h; optical yield given as %ee; enantioselective reaction;

DOI:10.1039/c1ob06319g

upstream raw materials:

benzoyl chloride

Downstream raw materials:

C₉H₁₀⁽²⁾HNO₃

C₁₉H₂₀⁽²⁾HNO₄

(S)-m-tyrosine

C₁₉H₂₁NO₄