di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

Base Information

Chemical Name:di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide
CAS No.:359643-67-7
Molecular Formula:C₆₄H₈₂O₈S₅
Molecular Weight:1139.68
Hs Code.:

Synonyms:di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

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Chemical Property of di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

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Technology Process of di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

There total 7 articles about di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: aqueous 1M-HCl

: 359010-66-5
4-bromo-3-methyl-2-butenyl sulfide

: 359010-62-1
1,5-di(phenylsulfonyl)-3,7,11-trimethyl-2,6,10-dodecatriene

: 359643-67-7
di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

: 56691-80-6
geranyl phenyl sulfone

: 359643-67-7
di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

2: 75 percent / LiNbMoO₆; H₂O₂ / methanol

3: 89 percent / n-BuLi / tetrahydrofuran / -78 °C

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; In tetrahydrofuran; methanol;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: 57282-70-9
(E)-4-hydroxy-3-methyl-2-butenyl phenyl sulfide

: 359643-67-7
di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / PBr₃ / diethyl ether

2: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

3: 75 percent / LiNbMoO₆; H₂O₂ / methanol

4: 89 percent / n-BuLi / tetrahydrofuran / -78 °C

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; phosphorus tribromide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E