Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

Base Information

Chemical Name:Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone
CAS No.:359643-74-6
Molecular Formula:C₆₄H₈₂O₁₀S₅
Molecular Weight:1171.68
Hs Code.:

Synonyms:Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

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Chemical Property of Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

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Technology Process of Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

There total 9 articles about Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 359643-67-7
di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfide

: 359643-74-6
Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

Guidance literature:: With LiNbMoO₆; dihydrogen peroxide; In methanol;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: 56691-80-6
geranyl phenyl sulfone

: 359643-74-6
Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

2: 75 percent / LiNbMoO₆; H₂O₂ / methanol

3: 89 percent / n-BuLi / tetrahydrofuran / -78 °C

4: 72 percent / LiNbMoO₆; H₂O₂ / methanol

With n-butyllithium; LiNbMoO₆; dihydrogen peroxide; In tetrahydrofuran; methanol;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E

Reference yield:

: 108-98-5
thiophenol

: 359643-74-6
Di(5,9-di(phenylsulfonyl)-3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenyl) sulfone

Guidance literature:: Multi-step reaction with 6 steps

1: CuI / dimethylformamide

2: 85 percent / PBr₃ / diethyl ether

3: 93 percent / n-BuLi / tetrahydrofuran / -78 °C

4: 75 percent / LiNbMoO₆; H₂O₂ / methanol

5: 89 percent / n-BuLi / tetrahydrofuran / -78 °C

6: 72 percent / LiNbMoO₆; H₂O₂ / methanol

With copper(l) iodide; n-butyllithium; LiNbMoO₆; dihydrogen peroxide; phosphorus tribromide; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/1521-3773(20011001)40:19<3627::AID-ANIE3627>3.0.CO;2-E