(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

Base Information

Chemical Name:(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine
CAS No.:1403828-84-1
Molecular Formula:C₁₈H₂₆BrNO₂
Molecular Weight:368.314
Hs Code.:

Synonyms:(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

Suppliers and Price of (2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

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Technology Process of (2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

There total 1 articles about (2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1403828-83-0
2-(2-bromocyclohex-2-enylamino)-2-methylpropan-1-ol

: 824-94-2
p-methoxybenzyl chloride

: 1403828-84-1
(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/anie.201205403

Reference yield: 83.0%

: 1403828-84-1
(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

: 407-25-0
trifluoroacetic anhydride

: 1403828-85-2
N-(2-bromocyclohex-2-enyl)-2,2,2-trifluoro-N-[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]acetamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1002/anie.201205403

Reference yield:

: 1403828-84-1
(2-bromocyclohex-2-enyl)[2-(4-methoxybenzyloxy)-1,1-dimethylethyl]amine

: 2,2,2-trifluoro-1-[2-(4-methoxybenzyloxymethyl)-2-methyl-2,3,5,6,7,7a-hexahydroindol-1-yl]-ethanone

: 2,2,2-trifluoro-1-[2-(4-methoxybenzyloxymethyl)-2-methyl-2,3,5,6,7,7a-hexahydroindol-1-yl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 6 h / 20 °C

2: palladium diacetate; tricyclohexylphosphine tetrafluoroborate; rubidium carbonate; Trimethylacetic acid / toluene / 20 - 120 °C

With rubidium carbonate; pyridine; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid; In dichloromethane; toluene;
DOI:10.1002/anie.201205403