N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

Base Information

Chemical Name:N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide
CAS No.:1362244-08-3
Molecular Formula:C₂₂H₂₁NO₄
Molecular Weight:363.413
Hs Code.:

Synonyms:N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

Chemical Property:

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Technology Process of N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

There total 6 articles about N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1362244-04-9
2-hydroxy-N-(3-(1-hydroxynaphthalen-2-yl)-2,2-dimethylpropyl)benzamide

: 1362244-08-3
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

Guidance literature:: With potassium nitrososulfonate; In methanol; water; N,N-dimethyl-formamide; at 20 ℃; for 7h;
DOI:10.1016/j.ejmech.2012.01.020

Reference yield:

: 1362244-00-5
2-methoxy-N-(3-(1-methoxynaphthalen-2-yl)-2,2-dimethylpropyl)benzamide

: 1362244-08-3
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / 2.03 h / 0 - 20 °C

1.2: 0 °C

2.1: potassium nitrososulfonate / methanol; water; N,N-dimethyl-formamide / 7 h / 20 °C

With potassium nitrososulfonate; boron tribromide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.020

Reference yield:

: 1362243-97-7
methyl 2-((1-methoxynaphthalen-2-yl) methyl)-2-methylpropanenitrile

: 1362244-08-3
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.08 h / 0 - 20 °C

1.2: 20 °C

2.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / methanol / 1 h / 20 °C

3.1: boron tribromide / dichloromethane / 2.03 h / 0 - 20 °C

3.2: 0 °C

4.1: potassium nitrososulfonate / methanol; water; N,N-dimethyl-formamide / 7 h / 20 °C

With lithium aluminium tetrahydride; potassium nitrososulfonate; boron tribromide; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.020