N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

Base Information

Chemical Name:N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide
CAS No.:1362244-19-6
Molecular Formula:C₂₃H₂₃NO₄
Molecular Weight:377.44
Hs Code.:

Synonyms:N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

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Chemical Property of N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

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Technology Process of N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

There total 6 articles about N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1362244-08-3
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide

: 77-78-1
dimethyl sulfate

: 1362244-19-6
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

Guidance literature:: N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-hydroxybenzamide; With potassium carbonate; In acetone; at 20 ℃;

dimethyl sulfate; In acetone; at 20 ℃; for 8h;
DOI:10.1016/j.ejmech.2012.01.020

Reference yield:

: 1362244-00-5
2-methoxy-N-(3-(1-methoxynaphthalen-2-yl)-2,2-dimethylpropyl)benzamide

: 1362244-19-6
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane / 2.03 h / 0 - 20 °C

1.2: 0 °C

2.1: potassium nitrososulfonate / methanol; water; N,N-dimethyl-formamide / 7 h / 20 °C

3.1: potassium carbonate / acetone / 20 °C

3.2: 8 h / 20 °C

With potassium nitrososulfonate; boron tribromide; potassium carbonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2012.01.020

Reference yield:

: 1362244-04-9
2-hydroxy-N-(3-(1-hydroxynaphthalen-2-yl)-2,2-dimethylpropyl)benzamide

: 1362244-19-6
N-(3-(1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2,2-dimethylpropyl)-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium nitrososulfonate / methanol; water; N,N-dimethyl-formamide / 7 h / 20 °C

2.1: potassium carbonate / acetone / 20 °C

2.2: 8 h / 20 °C

With potassium nitrososulfonate; potassium carbonate; In methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2012.01.020