Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2)

Base Information

• Chemical Name: Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2)
• CAS No.: 477849-06-2
• Molecular Formula: C₂₆H₂₂IO₂P₂Rh
• Molecular Weight: 658.217

Synonyms:Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2)

Chemical Property of Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2)

Chemical Property:

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Technology Process of Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2)

There total 1 articles about Rh(CO)I((C₆H₅)2PCH₂P(O)(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

[Rh(CO)2(μ-I)]2 + bis(diphenylphosphino)methane monooxide (23176-18-3) → Rh(CO)I((C6H5)2PCH2P(O)(C6H5)2) (477849-06-2)

Guidance literature:

In dichloromethane; toluene; using Schlenk techniques; to (Rh(CO)2I)2 dissolved in toluene/CH2Cl2 added dropwise soln. of org. ligand in toluene; after 30 min ppt. filtered; washed (ether); dried (vac.); elem. anal.;

DOI:10.1021/ja0176191

Reference yield:

Rh(CO)I((C6H5)2PCH2P(O)(C6H5)2) (477849-06-2) + methyl iodide (74-88-4) → Rh(CO)(CH3)I2((C6H5)2PCH2P(O)(C6H5)2)

Guidance literature:

In dichloromethane; excess of MeI in CH2Cl2 added to solid metal complex at 25°C; not isolated; monitored by IR; Kinetics;

DOI:10.1021/ja0176191

Reference yield:

Rh(CO)I((C6H5)2PCH2P(O)(C6H5)2) (477849-06-2) + methyl iodide (74-88-4) → Rh(CO)(CH3)I2((C6H5)2PCH2P(O)(C6H5)2) + Rh(COCH3)I2((C6H5)2PCH2P(O)(C6H5)2)

Guidance literature:

In dichloromethane; under N2 atm. using Schlenk techniques; Rh complex dissolved in CH2Cl2; excess MeI added; not isolated; monitored by NMR, IR;

DOI:10.1021/ja0176191

upstream raw materials:

bis(diphenylphosphino)methane monooxide

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