C₃₈H₅₄O₃Si

Base Information

Chemical Name:C₃₈H₅₄O₃Si
CAS No.:1584133-11-8
Molecular Formula:C₃₈H₅₄O₃Si
Molecular Weight:586.93
Hs Code.:

C<sub>38</sub>H<sub>54</sub>O<sub>3</sub>Si

Synonyms:C₃₈H₅₄O₃Si

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Chemical Property of C₃₈H₅₄O₃Si

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Technology Process of C₃₈H₅₄O₃Si

There total 3 articles about C₃₈H₅₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1584133-07-2
C₃₈H₅₂O₃Si

: C₃₈H₅₄O₃Si

: 1584133-11-8
C₃₈H₅₄O₃Si

Guidance literature:: C₃₈H₅₂O₃Si; With diisobutylaluminium hydride; In dichloromethane; cyclohexane; at -78 ℃; for 0.583333h;

With rochelle salt; In dichloromethane; cyclohexane; water; at 20 ℃; for 1h; Overall yield = 100 %; Overall yield = 10 g;
DOI:10.1021/ol500727c

Reference yield:

: 77-60-1
tigogenin

: C₃₈H₅₄O₃Si

: 1584133-11-8
C₃₈H₅₄O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; sulfuric acid; iodine; peroxyacetic acid / acetic anhydride / 24 h / 20 °C

1.2: 12 h / 20 °C

2.1: 1H-imidazole; dmap / dichloromethane / 3.5 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 0.58 h / -78 °C

3.2: 1 h / 20 °C

With 1H-imidazole; dmap; peroxyacetic acid; sulfuric acid; iodine; diisobutylaluminium hydride; acetic acid; In dichloromethane; cyclohexane; acetic anhydride;
DOI:10.1021/ol500727c

Reference yield:

: 514-33-0
(16S,20S)-3β-hydroxy-23,24-bis-norcholano-22,16-lactone

: C₃₈H₅₄O₃Si

: 1584133-11-8
C₃₈H₅₄O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole; dmap / dichloromethane / 3.5 h / 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 0.58 h / -78 °C

2.2: 1 h / 20 °C

With 1H-imidazole; dmap; diisobutylaluminium hydride; In dichloromethane; cyclohexane;
DOI:10.1021/ol500727c