Technology Process of C41H52O7
There total 12 articles about C41H52O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; 2,4,6-trichlorobenzoyl chloride;
In
toluene;
at 23 ℃;
for 20h;
DOI:10.1002/ejoc.201200286
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: iodine; zinc / tetrahydrofuran / 2 h / Inert atmosphere; Reflux
2.1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C / Inert atmosphere
2.2: Rochelle's salt / -78 - 23 °C / Inert atmosphere
3.1: toluene / 16 h / 100 °C / Inert atmosphere
4.1: (1S)-10-camphorsulfonic acid / dichloromethane / 25 h / 0 - 23 °C / Inert atmosphere; Molecular sieve
5.1: sodium hydroxide / ethanol; water / 0 - 23 °C
5.2: pH 3
6.1: triethylamine / toluene / 1.5 h / 23 °C
7.1: dmap / toluene / 20 h
With
dmap; (1S)-10-camphorsulfonic acid; iodine; diisobutylaluminium hydride; triethylamine; sodium hydroxide; zinc;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;
3.1: Wittig reaction;
DOI:10.1021/ol201626h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene / 16 h / 100 °C / Inert atmosphere
2.1: (1S)-10-camphorsulfonic acid / dichloromethane / 25 h / 0 - 23 °C / Inert atmosphere; Molecular sieve
3.1: sodium hydroxide / ethanol; water / 0 - 23 °C
3.2: pH 3
4.1: triethylamine / toluene / 1.5 h / 23 °C
5.1: dmap / toluene / 20 h
With
dmap; (1S)-10-camphorsulfonic acid; triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; water; toluene;
1.1: Wittig reaction;
DOI:10.1021/ol201626h
