(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

Base Information

Chemical Name:(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol
CAS No.:119594-27-3
Molecular Formula:C₃₅H₅₄O₄Si
Molecular Weight:566.897
Hs Code.:

Synonyms:(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

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Chemical Property of (S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

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Technology Process of (S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

There total 7 articles about (S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119619-00-0
{(1S,2S,3R)-3-((S)-4-Benzyloxy-1-methyl-butyl)-1-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentylmethoxy}-tert-butyl-diphenyl-silane

: 119594-27-3
(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

Guidance literature:: With hydrogen; palladium dihydroxide; In ethanol; under 760 Torr; Ambient temperature;
DOI:10.1021/ja00189a069

Reference yield:

: 119594-26-2
{(1S,4S,5S)-4-((S)-4-Benzyloxy-1-methyl-butyl)-1-methyl-5-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopent-2-enylmethoxy}-tert-butyl-diphenyl-silane

: 119594-27-3
(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethyl acetate / 760 Torr / Ambient temperature

2: H₂ / Pd(OH)2 / ethanol / 760 Torr / Ambient temperature

With hydrogen; platinum(IV) oxide; palladium dihydroxide; In ethanol; ethyl acetate;
DOI:10.1021/ja00189a069

Reference yield:

: 119594-24-0
(S)-5-Benzyloxy-2-{(1S,4S,5S)-4-(tert-butyl-diphenyl-silanyloxymethyl)-4-methyl-5-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopent-2-enyl}-pentan-1-ol

: 119594-27-3
(S)-4-{(1R,2S,3S)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-2-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-cyclopentyl}-pentan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0 °C

2: LiAlH₄ / diethyl ether / Ambient temperature

3: H₂ / PtO₂ / ethyl acetate / 760 Torr / Ambient temperature

4: H₂ / Pd(OH)2 / ethanol / 760 Torr / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; triethylamine; platinum(IV) oxide; palladium dihydroxide; In diethyl ether; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00189a069