2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

Base Information

Chemical Name:2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine
CAS No.:1384216-39-0
Molecular Formula:C₁₅H₂₃BFNO₂
Molecular Weight:279.163
Hs Code.:

Synonyms:2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

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Chemical Property of 2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

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Technology Process of 2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

There total 2 articles about 2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 2341-21-1
2-fluoro-N,N-dimethylbenzylamine

: 73183-34-3
bis(pinacol)diborane

: 1384216-39-0
2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

Guidance literature:: With 2-(Aminomethyl)pyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In methyl cyclohexane; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol301635x

Reference yield:

: 446-48-0
o-fluorobenzyl bromide

: 1384216-39-0
2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 4 h / Inert atmosphere; Reflux

2: 2-(Aminomethyl)pyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / methyl cyclohexane / 16 h / 70 °C / Inert atmosphere

With 2-(Aminomethyl)pyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In ethanol; water; methyl cyclohexane;
DOI:10.1021/ol301635x

Reference yield: 46.0%

: 1384216-39-0
2-fluoro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N,N-dimethylbenzylamine

: 62-53-3
aniline

: 2-((dimethylamino)methyl)-3-fluoro-N-phenylaniline

Guidance literature:: With oxygen; copper(II) acetate monohydrate; In acetonitrile; at 80 ℃; for 2h; chemoselective reaction; Schlenk technique; Molecular sieve;
DOI:10.1021/acs.joc.5b01074