1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester

Base Information

• Chemical Name: 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester
• CAS No.: 1071157-71-5
• Molecular Formula: C₂₃H₃₃N₃O₆
• Molecular Weight: 447.532

Synonyms:1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester

Chemical Property of 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester

Chemical Property:

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Technology Process of 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester

There total 3 articles about 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-{[1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-phenyl}-meth-(E)-ylidene]-amino}-cyclopropanecarboxylic acid methyl ester → 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester (1071157-71-5)

Guidance literature:

With sodium cyanoborohydride; In ethanol; for 3h;

DOI:10.1021/jm00385a012

Reference yield:

methyl 1-aminocyclopropane-1-carboxylate (72784-43-1) → 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester (1071157-71-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.5 h

2: NaBH₃CN / ethanol / 3 h

With sodium cyanoborohydride; In ethanol;

DOI:10.1021/jm00385a012

Reference yield:

N-Cyclohexyl-N-methyl-4-(3-formyl-4-nitrophenyl)-oxybutyramide (94193-38-1) → 1-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-cyclopropanecarboxylic acid methyl ester (1071157-71-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.5 h

2: NaBH₃CN / ethanol / 3 h

With sodium cyanoborohydride; In ethanol;

DOI:10.1021/jm00385a012

upstream raw materials:

methyl 1-aminocyclopropane-1-carboxylate

N-Cyclohexyl-N-methyl-4-(3-formyl-4-nitrophenyl)-oxybutyramide

Downstream raw materials:

C₂₃H₃₀N₄O₃

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