2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide

Base Information

• Chemical Name: 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide
• CAS No.: 97669-55-1
• Molecular Formula: C₃₂H₃₀N₄O₄S₂
• Molecular Weight: 598.747

Synonyms:2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide

Chemical Property of 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide

Chemical Property:

Purity/Quality:

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Technology Process of 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide

There total 1 articles about 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol (111835-46-2) → 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide (97669-55-1)

Guidance literature:

With iodine; In ethanol; for 1h; Ambient temperature;

DOI:10.1007/BF00505906

Reference yield: 53.0%

2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide (97669-55-1) → 2,2'-bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methylpyridyl) disulfide (97651-33-7)

Guidance literature:

With nitric acid; for 0.333333h; Heating;

DOI:10.1007/BF00505906

Reference yield: 39.0%

piperidine (110-89-4) + 2,2'-Bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methyl-1,4-dihydropyridyl) Disulfide (97669-55-1) → 5-Cyano-2-methyl-4-phenyl-6-(piperidin-1-ylsulfanyl)-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester (97651-34-8) + piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol (111835-46-2)

Guidance literature:

In ethanol; for 0.166667h;

DOI:10.1007/BF00505906

upstream raw materials:

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol

Downstream raw materials:

5-Cyano-2-methyl-4-phenyl-6-(piperidin-1-ylsulfanyl)-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester

piperidinium salt of 6-methyl-4-phenyl-5-ethoxycarbonyl-3-cyano-1,4-dihydropyridine-2(1H)-thiol

2,2'-bis(3-cyano-4-phenyl-5-ethoxycarbonyl-6-methylpyridyl) disulfide

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