(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

Base Information

Chemical Name:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester
CAS No.:72704-07-5
Molecular Formula:C₂₂H₂₀O₆
Molecular Weight:380.397
Hs Code.:

Synonyms:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

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Chemical Property of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

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Technology Process of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

There total 4 articles about (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: acetic acid 4-(2-chlorocarbonylvinyl)phenyl ester

: 1202495-53-1
1-hydroxy-3-(4-acetoxyphenyl)-2-propen

: 72704-07-5
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

Guidance literature:: With dmap; triethylamine; at 0 ℃; for 1.5h;
DOI:10.1039/c3ra42818d

Reference yield:

: 27542-85-4,50363-92-3,15486-19-8
3-(4-acetoxyphenyl)acrylic acid

: 72704-07-5
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

2: triethylamine; dmap / 1.5 h / 0 °C

With dmap; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c3ra42818d

Reference yield:

: C₁₄H₁₄O₆

: 72704-07-5
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-phenyl)-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethyl acetate; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

2: triethylamine; dmap / 1.5 h / 0 °C

With dmap; sodium tetrahydroborate; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c3ra42818d