<(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

Base Information

Chemical Name:<(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane
CAS No.:154220-39-0
Molecular Formula:C₂₄H₃₂ClN₃O₅S₂
Molecular Weight:542.12
Hs Code.:

Synonyms:<(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

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Technology Process of <(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

There total 1 articles about <(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 95388-08-2
N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane

: 4635-59-0
4-Chlorobutanoyl chloride

: 154220-39-0
<(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

Guidance literature:: With triethylamine; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81895-0

Reference yield:

: 154220-39-0
<(N,N'-bis(p-toluenesulfonyl))-(N''-(4-chlorobutyryl))>-1,4,7-triazacyclononane

: 154220-43-6
1--4-butane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine, NaI / acetonitrile / 24 h / Heating

2: LiAlH₄ / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)81895-0