(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

Base Information

Chemical Name:(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate
CAS No.:884318-72-3
Molecular Formula:C₂₆H₂₉NO₂Se
Molecular Weight:466.482
Hs Code.:

Synonyms:(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

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Chemical Property of (2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

Chemical Property:

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Technology Process of (2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

There total 3 articles about (2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 884318-64-3
ethyl 2-((R)-1-phenylethylimino)-4-phenyl-3-(phenylselanyl)butanoate

: 884318-71-2
(2S,3S)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

: 884318-72-3
(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

Guidance literature:: With sodium cyanoborohydride; acetic acid; In ethanol; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2005.12.030

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 884318-72-3
(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄ / heptane; diethyl ether / 3.5 h / 0 - 20 °C

2: NaBH₃CN; AcOH / ethanol / 1 h / 0 °C

With titanium tetrachloride; sodium cyanoborohydride; acetic acid; In diethyl ether; ethanol; n-heptane;
DOI:10.1016/j.tet.2005.12.030

Reference yield:

: 200286-34-6
2-Oxo-4-phenyl-3-phenylselanyl-butyric acid ethyl ester

: 884318-72-3
(2R,3R)-ethyl 2-((R)-1-phenylethylamino)-4-phenyl-3-(phenylselanyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄ / heptane; diethyl ether / 3.5 h / 0 - 20 °C

2: NaBH₃CN; AcOH / ethanol / 1 h / 0 °C

With titanium tetrachloride; sodium cyanoborohydride; acetic acid; In diethyl ether; ethanol; n-heptane;
DOI:10.1016/j.tet.2005.12.030